Micro-pulling and shoulder expanding at cooled center
is a sapphire growth method, which is also called micro-pulling rotation
Kyropoulos. The is an improved method based on Kyropoulos Method and Pulling
Method by Institute of Composite Structures from the Harbin Institute of
Technology. It is used to grow large size crystal. Crystal growing system
includes control system, vacuum system, heating body, cooling system and
thermal protection systems. The following a picture, which is a schematic
shoulder cold heart to put the system trace Czochralski method, SAPMAC grown
single crystal, the outlook is usually pear-shaped, crystal diameter crucible
can grow to more than the inner diameter of the small size of 10 ~ 30mm. The
seed is processed into split shape, use seed clips at the bottom of the heat
exchanger. Rotating and pulling the heat exchanger can be accomplished seed
fixed, crystals, and the exchange interaction between the heat exchanger,
crystal and melt.

Cold Heart put the shoulder when trace Czochralski growth of sapphire crystals,
usually the entire crystal growth process can be divided into four control
phases, namely seeding, put the shoulder, and other tracks, annealing and
cooling phases. Seeding stage and put the shoulder is the use of adjusting heat
exchanger cooling capacity, appropriate with a certain reduction in heating
temperature (heating system can provide the crucible outer wall temperature)
way to achieve the crystal and put the shoulder necking control. At this time
the crystal growth rate and temperature gradient interface projecting large,
which is conducive to the use of larger discharge shoulders, reducing the
distance to put the shoulder to prevent flipping interface, while capable of
dislocation within the seed crystal defects such as the original fast from
Crystals spread to the crystal surface, effectively reducing defects within the
crystal content. Large temperature gradient also can increase the interface
crystal growth driving force, increase the stability of the interface. Until
crystals grow to the desired diameter size (cold shoulder put heart trace
Czochralski crystal diameter can grow from the inner wall of the crucible 1 ~
3cm), crystals begin Equal grow into other tracks stage. With grown crystal
size, heat exchanger efficiency of crystal growth decreases rapidly, so the
crystal enters Once diameter growth stage, mainly by reducing the heating
temperature(Crucible outer wall temperature of the heating system can provide)
to achieve crystal growth.
If there is any other question refer to tungsten crucible for
sapphire growth furnace, please feel free to contact us through the following
methods:
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Tel.:+86 592 512 9696
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